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Preparation and Characterization of In(OH)3:Eu Nanostructures Obtained by Microwave-Assisted Hydrothermal Method (pp.255-266) $100.00
Authors:  (Fabiana Villela da Motta, Ana Paula de Azevedo Marques, Carlos A. Paskocimas, Mauricio R.D. Bomio, Maria Fernanda C. Abreu, Máximo S. Li, Edson R. Leite, José A. Varela, Elson Longo, Laboratório de Síntese Química, Departamento de Engenharia de Materiais, Universidade Federal do Rio Grande do Norte, Natal, RN, Brazil, and others)
Abstract:
Crystalline europium-doped indium hydroxide (In(OH)3:Eu) nanostructures were prepared by a rapid and efficient Microwave-Assisted Hydrothermal (MAH) method. Nanostructures were obtained at a low temperature. FE-SEM images confirm that these samples are composed of 3D nanostructures. XRD, optical diffuse reflectance and photoluminescence (PL) measurements were used to characterize the products. Emission spectra of europium-doped indium hydroxide samples under excitation (350.7 nm) presented broad band emission referent to the indium hydroxide (In(OH)3) matrix and 5D0→7F0, 5D0→ 7F1, 5D0→ 7F2, 5D0→ 7F3 and 5D0→ 7F4 europium transitions at 582, 596, 618, 653 and 701 nm, respectively. Relative intensities of the Eu3+ emissions increased as the concentration of this ion increased from 0, 1, 2, 4 and 8 mol %, of Eu3+, but the luminescence is drastically quenched for the In(OH)3 matrix. 


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Preparation and Characterization of In(OH)3:Eu Nanostructures Obtained by Microwave-Assisted Hydrothermal Method (pp.255-266)